Title:Mechanically Activated Solid-State Synthesis of Phenylhydrazone Derivatives via High-Speed Ball Milling
Volume: 11
Issue: 8
Author(s): Xingyi Zhu, Yuanyuan Chen, Yuhe Chen, Jue Wang and Weike Su
Affiliation:
Keywords:
Ball milling, solid-state synthesis, phenylhydrazones, arenediazonium tetrafluoroborates, active methylene compounds.
Abstract: A series of phenylhydrazone derivatives was synthesized from arenediazonium tetrafluoroborates and active
methylene compounds under high-speed ball milling. The reaction occurred in the absence of the solvent and products
were obtained in good yield within short reaction times (no more than 30 min).