Abstract
A novel peptide complex was synthesized by a solid-solid reaction of glycyl-L-glutamine monohydrate and bismuth trichloride powders. The formula of the complex is (BiCl3)2[NH2CH2CONHCH(COOH)CH2CH2COOH·H2O]3. The crystal structure of the complex belongs to monoclinic system with the lattice parameters: a = 0.6914 nm, b = 0.7378 nm, c = 1.0005 nm, β = 194.1° . The characterization results of IR, Raman spectra and thermal analysis show that complex is dimer and unidentate coordination. Each bismuth atom and three chlorine atoms are coplanar in the complex.
Keywords: Peptide complex, bismuth trichloride, glycyl-L-glutamine, solid-solid reaction, synthesis, characterizations
Protein & Peptide Letters
Title: Synthesis and Characterization of Complex of Glycyl-L-Glutamine and Bismuth Trichloride
Volume: 15 Issue: 10
Author(s): Shaorong Luan, Yihua Zhu and Yuqing Jia
Affiliation:
Keywords: Peptide complex, bismuth trichloride, glycyl-L-glutamine, solid-solid reaction, synthesis, characterizations
Abstract: A novel peptide complex was synthesized by a solid-solid reaction of glycyl-L-glutamine monohydrate and bismuth trichloride powders. The formula of the complex is (BiCl3)2[NH2CH2CONHCH(COOH)CH2CH2COOH·H2O]3. The crystal structure of the complex belongs to monoclinic system with the lattice parameters: a = 0.6914 nm, b = 0.7378 nm, c = 1.0005 nm, β = 194.1° . The characterization results of IR, Raman spectra and thermal analysis show that complex is dimer and unidentate coordination. Each bismuth atom and three chlorine atoms are coplanar in the complex.
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Cite this article as:
Luan Shaorong, Zhu Yihua and Jia Yuqing, Synthesis and Characterization of Complex of Glycyl-L-Glutamine and Bismuth Trichloride, Protein & Peptide Letters 2008; 15 (10) . https://dx.doi.org/10.2174/092986608786071076
DOI https://dx.doi.org/10.2174/092986608786071076 |
Print ISSN 0929-8665 |
Publisher Name Bentham Science Publisher |
Online ISSN 1875-5305 |
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