Bu<sub>3</sub>SnH Assisted Radical Cyclization Towards the Synthesis of Pyrimidine-annulated Spirocyclic and [6,6] Fused Sulfur Heterocycles

ISSN: 1875-6255 (Online)
ISSN: 1570-1786 (Print)


Volume 11, 10 Issues, 2014


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Letters in Organic Chemistry

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Universidad de Alicante Apdo
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Bu3SnH Assisted Radical Cyclization Towards the Synthesis of Pyrimidine-annulated Spirocyclic and [6,6] Fused Sulfur Heterocycles

Author(s): K.C. Majumdar, P.K. Maji and S.K. Chattopadhayay

Affiliation: Department of Chemistry University of Kalyani, Kalyani-741235. W.B. India.

Abstract

Pyrimidine annulated sulfur heterocycles have been synthesized through tributyltin hydride-mediated radical reaction. This gave straight forward synthesis of tricyclic compound as well as spiro heterocyclic compounds. The reactions have been simple, straight forward and have been carried out in mild conditions.




Keywords: 5-exo-Cyclisation, , 6-endo Cyclization, AIBN, Pyrimidine, sulfur heterocycles, Tributyltin hydride, Radical reaction.

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Article Details

Volume: 11
Issue Number: 7
First Page: 487
Last Page: 492
Page Count: 6
DOI: 10.2174/1570178611666140318010053
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