Synthesis of Nanocrystalline Titania via Microwave-Assisted Homogeneous Hydrolysis Under Hydrothermal Conditions

ISSN: 2213-3364 (Online)
ISSN: 2213-3356 (Print)


Volume 1, 2 Issues, 2014






Current Microwave Chemistry

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Community Health Systems of South Texas (CHSST)
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Synthesis of Nanocrystalline Titania via Microwave-Assisted Homogeneous Hydrolysis Under Hydrothermal Conditions

Author(s): Egor A. Moskalenko, Alexey A. Sadovnikov, Alexander E. Baranchikov, Anastasia E. Goldt, Vladimir V. Kozik and Vladimir K. Ivanov

Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Leninsky, 31, Moscow, 119991, Russia.

Abstract

In this paper, we report on a new procedure for nanocrystalline titania synthesis using microwave-assisted homogeneous hydrolysis under hydrothermal conditions. We show that this synthetic procedure promotes formation of low-aggregated TiO2 powders with very high specific surface area (up to 240 m2–/g) and small particle size (5-7 nm), and that it hinders SO2 2– ions’ sorption on the surface of nanoparticles.




Keywords: Hexamethylenetetramine, homogeneous hydrolysis, nanocrystalline materials, microwave-hydrothermal synthesis, titania.

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Article Details

Volume: 1
Issue Number: 2
First Page: 81
Last Page: 86
Page Count: 6
DOI: 10.2174/2213335601666140404163607
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